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Article: Determination of iodate in iodized salt by reversed-phase high-performance liquid chromatography with UV detection

TitleDetermination of iodate in iodized salt by reversed-phase high-performance liquid chromatography with UV detection
Authors
KeywordsColumn liquid chromatography
Lodate in iodized salt
Issue Date2004
PublisherFriedr Vieweg und Sohn Verlagsgesellschaft mbH. The Journal's web site is located at http://www.elsevier.com/locate/chromatographia
Citation
Chromatographia, 2004, v. 60 n. 11-12, p. 721-723 How to Cite?
AbstractA method for the determination of iodate was developed by reversed-phase high-performance liquid chromatography with UV detection. Iodate was converted to iodine, which was separated from the matrix using a reversed-phase Ultrasphere C18 column (250 x 4.6 mm, 5 μm) with methanol-1 mmol L-1 H3PO4 (20:80, v/v) as mobile phase at 1.00 mL min-1 and UV detection at 224 nm. The calibration graph was linear from 0.05 μg mL-1 to 5.00μg mL-1 for iodine with a correlation coefficient of 0.9994 (n = 7). The detection limit was 0.01 μg mL-1. The method was successfully applied to the determination of iodate in iodized salt. The recovery was from 96% to 101% and the relative standard deviation was in the range of 1.5% to 2.9%.
Persistent Identifierhttp://hdl.handle.net/10722/73423
ISSN
2023 Impact Factor: 1.2
2023 SCImago Journal Rankings: 0.301
ISI Accession Number ID
References

 

DC FieldValueLanguage
dc.contributor.authorXu, XRen_HK
dc.contributor.authorLi, HBen_HK
dc.contributor.authorGu, JDen_HK
dc.contributor.authorPaeng, KJen_HK
dc.date.accessioned2010-09-06T06:51:08Z-
dc.date.available2010-09-06T06:51:08Z-
dc.date.issued2004en_HK
dc.identifier.citationChromatographia, 2004, v. 60 n. 11-12, p. 721-723en_HK
dc.identifier.issn0009-5893en_HK
dc.identifier.urihttp://hdl.handle.net/10722/73423-
dc.description.abstractA method for the determination of iodate was developed by reversed-phase high-performance liquid chromatography with UV detection. Iodate was converted to iodine, which was separated from the matrix using a reversed-phase Ultrasphere C18 column (250 x 4.6 mm, 5 μm) with methanol-1 mmol L-1 H3PO4 (20:80, v/v) as mobile phase at 1.00 mL min-1 and UV detection at 224 nm. The calibration graph was linear from 0.05 μg mL-1 to 5.00μg mL-1 for iodine with a correlation coefficient of 0.9994 (n = 7). The detection limit was 0.01 μg mL-1. The method was successfully applied to the determination of iodate in iodized salt. The recovery was from 96% to 101% and the relative standard deviation was in the range of 1.5% to 2.9%.en_HK
dc.languageengen_HK
dc.publisherFriedr Vieweg und Sohn Verlagsgesellschaft mbH. The Journal's web site is located at http://www.elsevier.com/locate/chromatographiaen_HK
dc.relation.ispartofChromatographiaen_HK
dc.subjectColumn liquid chromatographyen_HK
dc.subjectLodate in iodized salten_HK
dc.titleDetermination of iodate in iodized salt by reversed-phase high-performance liquid chromatography with UV detectionen_HK
dc.typeArticleen_HK
dc.identifier.openurlhttp://library.hku.hk:4550/resserv?sid=HKU:IR&issn=0009-5893&volume=60&spage=721&epage=723&date=2004&atitle=Determination+of+iodate+in+iodized+salt+by+Reversed-phase+High-Performance+Liquid+Chromatography+with+UV+detectionen_HK
dc.identifier.emailGu, JD: jdgu@hkucc.hku.hken_HK
dc.identifier.authorityGu, JD=rp00701en_HK
dc.description.naturelink_to_subscribed_fulltext-
dc.identifier.doi10.1365/s10337-004-0430-6en_HK
dc.identifier.scopuseid_2-s2.0-12144257648en_HK
dc.identifier.hkuros98025en_HK
dc.relation.referenceshttp://www.scopus.com/mlt/select.url?eid=2-s2.0-12144257648&selection=ref&src=s&origin=recordpageen_HK
dc.identifier.volume60en_HK
dc.identifier.issue11-12en_HK
dc.identifier.spage721en_HK
dc.identifier.epage723en_HK
dc.identifier.isiWOS:000225815500019-
dc.publisher.placeGermanyen_HK
dc.identifier.scopusauthoridXu, XR=7405293882en_HK
dc.identifier.scopusauthoridLi, HB=25649944400en_HK
dc.identifier.scopusauthoridGu, JD=7403129601en_HK
dc.identifier.scopusauthoridPaeng, KJ=7003279415en_HK
dc.identifier.issnl0009-5893-

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