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- Publisher Website: 10.1016/j.aca.2007.05.032
- Scopus: eid_2-s2.0-34250615538
- PMID: 17586124
- WOS: WOS:000248111100016
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Article: Simultaneous determination of 17 ginsenosides in rat urine by ultra performance liquid chromatography-mass spectrometry with solid-phase extraction
| Title | Simultaneous determination of 17 ginsenosides in rat urine by ultra performance liquid chromatography-mass spectrometry with solid-phase extraction |
|---|---|
| Authors | |
| Keywords | Ginsenoside Rat urine Saponin Solid-phase extraction Ultra performance liquid chromatography-mass spectrometry |
| Issue Date | 2007 |
| Citation | Analytica Chimica Acta, 2007, v. 594, n. 2, p. 265-273 How to Cite? |
| Abstract | A rapid analytical method for quantifying 17 ginsenosides in rat urine by ultra performance liquid chromatography (UPLC) coupled to electrospray ionization mass spectrometry (ESI-MS) is described. All analytes were extracted by solid-phase extraction optimized to obtain good recovery and quantified using digoxin as an internal standard. ESI-MS was optimized for different cone voltages at positive ionization mode to allow simultaneous analysis of all analytes in a relatively short time. Qualitative methodological considerations, including the linear range, precision, limit of quantification, limit of detection, recovery and sensitivity are also provided. © 2007 Elsevier B.V. All rights reserved. |
| Persistent Identifier | http://hdl.handle.net/10722/342312 |
| ISSN | 2023 Impact Factor: 5.7 2023 SCImago Journal Rankings: 0.998 |
| ISI Accession Number ID |
| DC Field | Value | Language |
|---|---|---|
| dc.contributor.author | Wang, Xiaoyan | - |
| dc.contributor.author | Zhao, Tie | - |
| dc.contributor.author | Gao, Xianfu | - |
| dc.contributor.author | Dan, Mo | - |
| dc.contributor.author | Zhou, Mingmei | - |
| dc.contributor.author | Jia, Wei | - |
| dc.date.accessioned | 2024-04-17T07:02:53Z | - |
| dc.date.available | 2024-04-17T07:02:53Z | - |
| dc.date.issued | 2007 | - |
| dc.identifier.citation | Analytica Chimica Acta, 2007, v. 594, n. 2, p. 265-273 | - |
| dc.identifier.issn | 0003-2670 | - |
| dc.identifier.uri | http://hdl.handle.net/10722/342312 | - |
| dc.description.abstract | A rapid analytical method for quantifying 17 ginsenosides in rat urine by ultra performance liquid chromatography (UPLC) coupled to electrospray ionization mass spectrometry (ESI-MS) is described. All analytes were extracted by solid-phase extraction optimized to obtain good recovery and quantified using digoxin as an internal standard. ESI-MS was optimized for different cone voltages at positive ionization mode to allow simultaneous analysis of all analytes in a relatively short time. Qualitative methodological considerations, including the linear range, precision, limit of quantification, limit of detection, recovery and sensitivity are also provided. © 2007 Elsevier B.V. All rights reserved. | - |
| dc.language | eng | - |
| dc.relation.ispartof | Analytica Chimica Acta | - |
| dc.subject | Ginsenoside | - |
| dc.subject | Rat urine | - |
| dc.subject | Saponin | - |
| dc.subject | Solid-phase extraction | - |
| dc.subject | Ultra performance liquid chromatography-mass spectrometry | - |
| dc.title | Simultaneous determination of 17 ginsenosides in rat urine by ultra performance liquid chromatography-mass spectrometry with solid-phase extraction | - |
| dc.type | Article | - |
| dc.description.nature | link_to_subscribed_fulltext | - |
| dc.identifier.doi | 10.1016/j.aca.2007.05.032 | - |
| dc.identifier.pmid | 17586124 | - |
| dc.identifier.scopus | eid_2-s2.0-34250615538 | - |
| dc.identifier.volume | 594 | - |
| dc.identifier.issue | 2 | - |
| dc.identifier.spage | 265 | - |
| dc.identifier.epage | 273 | - |
| dc.identifier.isi | WOS:000248111100016 | - |