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- Scopus: eid_2-s2.0-24344500775
- PMID: 15575207
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Article: Determination of active anthraquinones in Rheum and its tea preparations by micellar electrokinetic capillary electrophoresis
Title | Determination of active anthraquinones in Rheum and its tea preparations by micellar electrokinetic capillary electrophoresis |
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Authors | |
Keywords | Aloe-emodin Anthraquinones Capillary electrophoresis Emodin Qinghai Wild Dahuang Tea Rhein Rheum |
Issue Date | 2004 |
Citation | Zhongguo Zhongyao Zazhi, 2004, v. 29, n. 9, p. 873 How to Cite? |
Abstract | Objective: To establish an instant determination method of emodin, aloe-emodin and rhein, from Rheum, and one of their preparations, Qinghai Wild Dahuang Tea, by micellar electrokinetic capillary electrophoresis for the first time. Method: Separation was carried out in an uncoated fused silica capillary (75 μm x 50.0 cm). Meanwhile, a running voltage 20 kV, 15.0 mmol·L-1 borax buffer with 30.0 mmol·L-1 SDS and 10% ethanol (pH 9.60) and a UV detector at 254 nm were adopted. Result: The linear calibration rang was 4-120 mg·L-1 (r = 0.992 1) for emodin, 10-200 mg·L-1 (r = 0.997 0) for aloe-emodin, and 2-100 mg·L-1 (r = 0.997 1) for rhein, respectively. Under the optimum conditions, the relative standard deviation (RSD) values (n = 6) for the migration time and the peak area of each peak were 0.59%-0.80%, 1.30%-3.22%, respectively. The contents of the analytes were easily determined with recoveries ranging from 97.6%-102.3%. Conclusion: The method is proved to be simple, rapid and accurate, and can be used for the quality control of medicinal herb, Rheum, and its tea preparation. |
Persistent Identifier | http://hdl.handle.net/10722/342279 |
ISSN | 2023 SCImago Journal Rankings: 0.206 |
DC Field | Value | Language |
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dc.contributor.author | Zheng, Wen Jie | - |
dc.contributor.author | Chen, Xing Guo | - |
dc.contributor.author | Jia, Wei | - |
dc.date.accessioned | 2024-04-17T07:02:39Z | - |
dc.date.available | 2024-04-17T07:02:39Z | - |
dc.date.issued | 2004 | - |
dc.identifier.citation | Zhongguo Zhongyao Zazhi, 2004, v. 29, n. 9, p. 873 | - |
dc.identifier.issn | 1001-5302 | - |
dc.identifier.uri | http://hdl.handle.net/10722/342279 | - |
dc.description.abstract | Objective: To establish an instant determination method of emodin, aloe-emodin and rhein, from Rheum, and one of their preparations, Qinghai Wild Dahuang Tea, by micellar electrokinetic capillary electrophoresis for the first time. Method: Separation was carried out in an uncoated fused silica capillary (75 μm x 50.0 cm). Meanwhile, a running voltage 20 kV, 15.0 mmol·L-1 borax buffer with 30.0 mmol·L-1 SDS and 10% ethanol (pH 9.60) and a UV detector at 254 nm were adopted. Result: The linear calibration rang was 4-120 mg·L-1 (r = 0.992 1) for emodin, 10-200 mg·L-1 (r = 0.997 0) for aloe-emodin, and 2-100 mg·L-1 (r = 0.997 1) for rhein, respectively. Under the optimum conditions, the relative standard deviation (RSD) values (n = 6) for the migration time and the peak area of each peak were 0.59%-0.80%, 1.30%-3.22%, respectively. The contents of the analytes were easily determined with recoveries ranging from 97.6%-102.3%. Conclusion: The method is proved to be simple, rapid and accurate, and can be used for the quality control of medicinal herb, Rheum, and its tea preparation. | - |
dc.language | eng | - |
dc.relation.ispartof | Zhongguo Zhongyao Zazhi | - |
dc.subject | Aloe-emodin | - |
dc.subject | Anthraquinones | - |
dc.subject | Capillary electrophoresis | - |
dc.subject | Emodin | - |
dc.subject | Qinghai Wild Dahuang Tea | - |
dc.subject | Rhein | - |
dc.subject | Rheum | - |
dc.title | Determination of active anthraquinones in Rheum and its tea preparations by micellar electrokinetic capillary electrophoresis | - |
dc.type | Article | - |
dc.description.nature | link_to_subscribed_fulltext | - |
dc.identifier.pmid | 15575207 | - |
dc.identifier.scopus | eid_2-s2.0-24344500775 | - |
dc.identifier.volume | 29 | - |
dc.identifier.issue | 9 | - |
dc.identifier.spage | 873 | - |
dc.identifier.epage | - |