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Article: Synthesis of 2-pyridone-fused 2,2′-bipyridine derivatives. An unexpectedly complex solid state structure of 3,6-dimethyl-9H-4,5,9- triazaphenanthren-10-one
Title | Synthesis of 2-pyridone-fused 2,2′-bipyridine derivatives. An unexpectedly complex solid state structure of 3,6-dimethyl-9H-4,5,9- triazaphenanthren-10-one |
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Authors | |
Issue Date | 2005 |
Citation | Organic and Biomolecular Chemistry, 2005, v. 3, n. 6, p. 996-1001 How to Cite? |
Abstract | 2-Pyridone-fused 2,2′-bipyridine derivatives 1a and 1b were synthesised. X-Ray diffraction analysis of 1b revealed a highly complex solid state structure with a disordered molecule imbedded in a channel structure formed by a centrosymmetric lattice of hexagonally packed, hydrogen bonded columns. The columns are assembled from three symmetry independent molecules. Dimerisation of the self-complementary cis-amide hydrogen bond motif is overridden by the fulfilment of the proton coordination ability of the phenanthroline nitrogens in accordance with Etter's rules of hydrogen bond priorities. © The Royal Society of Chemistry 2005. |
Persistent Identifier | http://hdl.handle.net/10722/341071 |
ISSN | 2023 Impact Factor: 2.9 2023 SCImago Journal Rankings: 0.607 |
ISI Accession Number ID |
DC Field | Value | Language |
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dc.contributor.author | Jónsson, Stefán | - |
dc.contributor.author | Arribas, Carlos Solano | - |
dc.contributor.author | Wendt, Ola F. | - |
dc.contributor.author | Siegel, Jay S. | - |
dc.contributor.author | Wärnmark, Kenneth | - |
dc.date.accessioned | 2024-03-13T08:39:55Z | - |
dc.date.available | 2024-03-13T08:39:55Z | - |
dc.date.issued | 2005 | - |
dc.identifier.citation | Organic and Biomolecular Chemistry, 2005, v. 3, n. 6, p. 996-1001 | - |
dc.identifier.issn | 1477-0520 | - |
dc.identifier.uri | http://hdl.handle.net/10722/341071 | - |
dc.description.abstract | 2-Pyridone-fused 2,2′-bipyridine derivatives 1a and 1b were synthesised. X-Ray diffraction analysis of 1b revealed a highly complex solid state structure with a disordered molecule imbedded in a channel structure formed by a centrosymmetric lattice of hexagonally packed, hydrogen bonded columns. The columns are assembled from three symmetry independent molecules. Dimerisation of the self-complementary cis-amide hydrogen bond motif is overridden by the fulfilment of the proton coordination ability of the phenanthroline nitrogens in accordance with Etter's rules of hydrogen bond priorities. © The Royal Society of Chemistry 2005. | - |
dc.language | eng | - |
dc.relation.ispartof | Organic and Biomolecular Chemistry | - |
dc.title | Synthesis of 2-pyridone-fused 2,2′-bipyridine derivatives. An unexpectedly complex solid state structure of 3,6-dimethyl-9H-4,5,9- triazaphenanthren-10-one | - |
dc.type | Article | - |
dc.description.nature | link_to_subscribed_fulltext | - |
dc.identifier.doi | 10.1039/b417485b | - |
dc.identifier.scopus | eid_2-s2.0-16244378225 | - |
dc.identifier.volume | 3 | - |
dc.identifier.issue | 6 | - |
dc.identifier.spage | 996 | - |
dc.identifier.epage | 1001 | - |
dc.identifier.isi | WOS:000227454700008 | - |