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Article: Isochronous and Anisochronous O-Methylene Protons in Cyclic and Acyclic Acetals

TitleIsochronous and Anisochronous O-Methylene Protons in Cyclic and Acyclic Acetals
Authors
Grindley, T. B.Stoddart, J. F.Szarek, W. A.
Issue Date1969
Citation
Journal of the American Chemical Society, 1969, v. 91, n. 17, p. 4722-4724 How to Cite?
DOI: http://dx.doi.org/10.1021/ja01045a024
AbstractConfigurational assignments are made to some cyclic and acyclic acetals on the basis of the nature of the signals for their O-methylene protons in their pmr spectra. The three known 4,5: 9,10-biscyclohexano-1,3,6,8-tetraoxacyclodecanes are assigned the trans-syn-trans, trans-anti-trans, and cis-anti-cis configurations and the di-(trans-2-hydroxycyclohexyloxy)methanes with mp 80-82° and mp 102.5-103.5° are assigned to the meso form and dl modification, respectively. © 1969, American Chemical Society. All rights reserved.
Persistent Identifierhttp://hdl.handle.net/10722/332723
ISSN
0002-7863
2023 Impact Factor: 14.4
2023 SCImago Journal Rankings: 5.489

 

DC FieldValueLanguage
dc.contributor.authorGrindley, T. B.-
dc.contributor.authorStoddart, J. F.-
dc.contributor.authorSzarek, W. A.-
dc.date.accessioned2023-10-06T05:13:46Z-
dc.date.available2023-10-06T05:13:46Z-
dc.date.issued1969-
dc.identifier.citationJournal of the American Chemical Society, 1969, v. 91, n. 17, p. 4722-4724-
dc.identifier.issn0002-7863-
dc.identifier.urihttp://hdl.handle.net/10722/332723-
dc.description.abstractConfigurational assignments are made to some cyclic and acyclic acetals on the basis of the nature of the signals for their O-methylene protons in their pmr spectra. The three known 4,5: 9,10-biscyclohexano-1,3,6,8-tetraoxacyclodecanes are assigned the trans-syn-trans, trans-anti-trans, and cis-anti-cis configurations and the di-(trans-2-hydroxycyclohexyloxy)methanes with mp 80-82° and mp 102.5-103.5° are assigned to the meso form and dl modification, respectively. © 1969, American Chemical Society. All rights reserved.-
dc.languageeng-
dc.relation.ispartofJournal of the American Chemical Society-
dc.titleIsochronous and Anisochronous O-Methylene Protons in Cyclic and Acyclic Acetals-
dc.typeArticle-
dc.description.naturelink_to_subscribed_fulltext-
dc.identifier.doi10.1021/ja01045a024-
dc.identifier.scopuseid_2-s2.0-33947301078-
dc.identifier.volume91-
dc.identifier.issue17-
dc.identifier.spage4722-
dc.identifier.epage4724-
dc.identifier.eissn1520-5126-

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