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Article: High-resolution 13C N.M.R. spectroscopy and x-ray crystallography of complexes formed by NN′-dimethyl-1,7-diaza-4,10- dioxacyclododecane

TitleHigh-resolution <sup>13</sup>C N.M.R. spectroscopy and x-ray crystallography of complexes formed by NN′-dimethyl-1,7-diaza-4,10- dioxacyclododecane
Authors
Metcalfe, Janet C.Stoddart, J. FraserJones, GeraintHull, William E.Atkinson, AnaKerr, Ian S.Williams, David J.
Issue Date1980
Citation
Journal of the Chemical Society, Chemical Communications, 1980, n. 12, p. 540-543 How to Cite?
DOI: http://dx.doi.org/10.1039/C39800000540
AbstractResults obtained from an X-ray crystal structure determination of the 1:1 complex formed between NN′-dimethyl-1,7-diaza-4,10-dioxacyclododecane (1) and benzylammonium thiocyanate and dynamic 13C n m r spectroscopy in CD2Cl2 of the 1:1 complex formed between (1) and (S)-α-phenylethylammonium perchlorate vindicate the constitutional and configurational validity of two-point binding with syn stereochemistry between the host and guest species but indicate that conformational isomerism can occur within the host species of such complexes.
Persistent Identifierhttp://hdl.handle.net/10722/332599
ISSN
0022-4936
ISI Accession Number ID
WOS:A1980JY26300003

 

DC FieldValueLanguage
dc.contributor.authorMetcalfe, Janet C.-
dc.contributor.authorStoddart, J. Fraser-
dc.contributor.authorJones, Geraint-
dc.contributor.authorHull, William E.-
dc.contributor.authorAtkinson, Ana-
dc.contributor.authorKerr, Ian S.-
dc.contributor.authorWilliams, David J.-
dc.date.accessioned2023-10-06T05:12:46Z-
dc.date.available2023-10-06T05:12:46Z-
dc.date.issued1980-
dc.identifier.citationJournal of the Chemical Society, Chemical Communications, 1980, n. 12, p. 540-543-
dc.identifier.issn0022-4936-
dc.identifier.urihttp://hdl.handle.net/10722/332599-
dc.description.abstractResults obtained from an X-ray crystal structure determination of the 1:1 complex formed between NN′-dimethyl-1,7-diaza-4,10-dioxacyclododecane (1) and benzylammonium thiocyanate and dynamic 13C n m r spectroscopy in CD2Cl2 of the 1:1 complex formed between (1) and (S)-α-phenylethylammonium perchlorate vindicate the constitutional and configurational validity of two-point binding with syn stereochemistry between the host and guest species but indicate that conformational isomerism can occur within the host species of such complexes.-
dc.languageeng-
dc.relation.ispartofJournal of the Chemical Society, Chemical Communications-
dc.titleHigh-resolution <sup>13</sup>C N.M.R. spectroscopy and x-ray crystallography of complexes formed by NN′-dimethyl-1,7-diaza-4,10- dioxacyclododecane-
dc.typeArticle-
dc.description.naturelink_to_subscribed_fulltext-
dc.identifier.doi10.1039/C39800000540-
dc.identifier.scopuseid_2-s2.0-1842776700-
dc.identifier.issue12-
dc.identifier.spage540-
dc.identifier.epage543-
dc.identifier.isiWOS:A1980JY26300003-

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