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Article: Electrochemical dissolution of tin in ethylene glycol monomethyl ether and direct hydrolysis of the electrolyte for preparation of nano-sized SnO 2

TitleElectrochemical dissolution of tin in ethylene glycol monomethyl ether and direct hydrolysis of the electrolyte for preparation of nano-sized SnO 2
Authors
Zhou, XFZhao, JFHe, HChu, DB
KeywordsNano-Sized Sno2
Organic Electrolysis Preparation
Sn(Och2ch2och3)4
Sol-Gel
Tin
Issue Date2004
Citation
Acta Physico - Chimica Sinica, 2004, v. 20 n. 12, p. 1472-1475 How to Cite?
AbstractMetallic tin was directly dissolved in ethylene glycol monomethyl ether and Sn (OCH2CH2OCH3)4 was obtained. The products were characterized by using FT-IR and Raman spectrum. The results show that direct electrochemical preparation of tin complexes has high current efficiency and electrolysis yield, and Sn(OCH2CH2OCH 3)4 can be dissolved in ethanol solution and directly used as sol-gel precursor for preparation of nanometer SnO2. The results also show that nano-sized SnO2 prepared by this method has tetragonal cassiterite structure with a narrow size distribution of (10.0 ± 0.4) nm.
Persistent Identifierhttp://hdl.handle.net/10722/182324
ISSN
1000-6818
2023 Impact Factor: 10.8
2023 SCImago Journal Rankings: 1.606
References
References in Scopus

 

DC FieldValueLanguage
dc.contributor.authorZhou, XFen_US
dc.contributor.authorZhao, JFen_US
dc.contributor.authorHe, Hen_US
dc.contributor.authorChu, DBen_US
dc.date.accessioned2013-04-23T08:18:53Z-
dc.date.available2013-04-23T08:18:53Z-
dc.date.issued2004en_US
dc.identifier.citationActa Physico - Chimica Sinica, 2004, v. 20 n. 12, p. 1472-1475en_US
dc.identifier.issn1000-6818en_US
dc.identifier.urihttp://hdl.handle.net/10722/182324-
dc.description.abstractMetallic tin was directly dissolved in ethylene glycol monomethyl ether and Sn (OCH2CH2OCH3)4 was obtained. The products were characterized by using FT-IR and Raman spectrum. The results show that direct electrochemical preparation of tin complexes has high current efficiency and electrolysis yield, and Sn(OCH2CH2OCH 3)4 can be dissolved in ethanol solution and directly used as sol-gel precursor for preparation of nanometer SnO2. The results also show that nano-sized SnO2 prepared by this method has tetragonal cassiterite structure with a narrow size distribution of (10.0 ± 0.4) nm.en_US
dc.languageengen_US
dc.relation.ispartofActa Physico - Chimica Sinicaen_US
dc.subjectNano-Sized Sno2en_US
dc.subjectOrganic Electrolysis Preparationen_US
dc.subjectSn(Och2ch2och3)4en_US
dc.subjectSol-Gelen_US
dc.subjectTinen_US
dc.titleElectrochemical dissolution of tin in ethylene glycol monomethyl ether and direct hydrolysis of the electrolyte for preparation of nano-sized SnO 2en_US
dc.typeArticleen_US
dc.identifier.emailZhao, JF: zhao0065@e.ntu.edu.sgen_US
dc.identifier.authorityZhao, JF=rp01745en_US
dc.description.naturelink_to_subscribed_fulltexten_US
dc.identifier.scopuseid_2-s2.0-11844279749en_US
dc.relation.referenceshttp://www.scopus.com/mlt/select.url?eid=2-s2.0-11844279749&selection=ref&src=s&origin=recordpageen_US
dc.identifier.volume20en_US
dc.identifier.issue12en_US
dc.identifier.spage1472en_US
dc.identifier.epage1475en_US
dc.publisher.placeChinaen_US
dc.identifier.scopusauthoridZhou, XF=7410092202en_US
dc.identifier.scopusauthoridZhao, JF=8393022100en_US
dc.identifier.scopusauthoridHe, H=55483699900en_US
dc.identifier.scopusauthoridChu, DB=7201734304en_US
dc.identifier.issnl1000-6818-

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