File Download
There are no files associated with this item.
Supplementary
-
Citations:
- Scopus: 0
- Appears in Collections:
Article: Electrochemical dissolution of tin in ethylene glycol monomethyl ether and direct hydrolysis of the electrolyte for preparation of nano-sized SnO 2
Title | Electrochemical dissolution of tin in ethylene glycol monomethyl ether and direct hydrolysis of the electrolyte for preparation of nano-sized SnO 2 |
---|---|
Authors | |
Keywords | Nano-Sized Sno2 Organic Electrolysis Preparation Sn(Och2ch2och3)4 Sol-Gel Tin |
Issue Date | 2004 |
Citation | Acta Physico - Chimica Sinica, 2004, v. 20 n. 12, p. 1472-1475 How to Cite? |
Abstract | Metallic tin was directly dissolved in ethylene glycol monomethyl ether and Sn (OCH2CH2OCH3)4 was obtained. The products were characterized by using FT-IR and Raman spectrum. The results show that direct electrochemical preparation of tin complexes has high current efficiency and electrolysis yield, and Sn(OCH2CH2OCH 3)4 can be dissolved in ethanol solution and directly used as sol-gel precursor for preparation of nanometer SnO2. The results also show that nano-sized SnO2 prepared by this method has tetragonal cassiterite structure with a narrow size distribution of (10.0 ± 0.4) nm. |
Persistent Identifier | http://hdl.handle.net/10722/182324 |
ISSN | 2023 Impact Factor: 10.8 2023 SCImago Journal Rankings: 1.606 |
References |
DC Field | Value | Language |
---|---|---|
dc.contributor.author | Zhou, XF | en_US |
dc.contributor.author | Zhao, JF | en_US |
dc.contributor.author | He, H | en_US |
dc.contributor.author | Chu, DB | en_US |
dc.date.accessioned | 2013-04-23T08:18:53Z | - |
dc.date.available | 2013-04-23T08:18:53Z | - |
dc.date.issued | 2004 | en_US |
dc.identifier.citation | Acta Physico - Chimica Sinica, 2004, v. 20 n. 12, p. 1472-1475 | en_US |
dc.identifier.issn | 1000-6818 | en_US |
dc.identifier.uri | http://hdl.handle.net/10722/182324 | - |
dc.description.abstract | Metallic tin was directly dissolved in ethylene glycol monomethyl ether and Sn (OCH2CH2OCH3)4 was obtained. The products were characterized by using FT-IR and Raman spectrum. The results show that direct electrochemical preparation of tin complexes has high current efficiency and electrolysis yield, and Sn(OCH2CH2OCH 3)4 can be dissolved in ethanol solution and directly used as sol-gel precursor for preparation of nanometer SnO2. The results also show that nano-sized SnO2 prepared by this method has tetragonal cassiterite structure with a narrow size distribution of (10.0 ± 0.4) nm. | en_US |
dc.language | eng | en_US |
dc.relation.ispartof | Acta Physico - Chimica Sinica | en_US |
dc.subject | Nano-Sized Sno2 | en_US |
dc.subject | Organic Electrolysis Preparation | en_US |
dc.subject | Sn(Och2ch2och3)4 | en_US |
dc.subject | Sol-Gel | en_US |
dc.subject | Tin | en_US |
dc.title | Electrochemical dissolution of tin in ethylene glycol monomethyl ether and direct hydrolysis of the electrolyte for preparation of nano-sized SnO 2 | en_US |
dc.type | Article | en_US |
dc.identifier.email | Zhao, JF: zhao0065@e.ntu.edu.sg | en_US |
dc.identifier.authority | Zhao, JF=rp01745 | en_US |
dc.description.nature | link_to_subscribed_fulltext | en_US |
dc.identifier.scopus | eid_2-s2.0-11844279749 | en_US |
dc.relation.references | http://www.scopus.com/mlt/select.url?eid=2-s2.0-11844279749&selection=ref&src=s&origin=recordpage | en_US |
dc.identifier.volume | 20 | en_US |
dc.identifier.issue | 12 | en_US |
dc.identifier.spage | 1472 | en_US |
dc.identifier.epage | 1475 | en_US |
dc.publisher.place | China | en_US |
dc.identifier.scopusauthorid | Zhou, XF=7410092202 | en_US |
dc.identifier.scopusauthorid | Zhao, JF=8393022100 | en_US |
dc.identifier.scopusauthorid | He, H=55483699900 | en_US |
dc.identifier.scopusauthorid | Chu, DB=7201734304 | en_US |
dc.identifier.issnl | 1000-6818 | - |