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Article: Oxidative addition of 2,2-dithiosalicylic acid to the cluster [Os3(CO)10(CH3CN)2]

TitleOxidative addition of 2,2-dithiosalicylic acid to the cluster [Os3(CO)10(CH3CN)2]
Authors
Issue Date1996
PublisherSpringer New York LLC. The Journal's web site is located at http://springerlink.metapress.com/openurl.asp?genre=journal&issn=1040-7278
Citation
Journal of Cluster Science, 1996, v. 7, p. 37-47 How to Cite?
AbstractThe reaction of 2,2'-dithiosalicylic acid with two equivalents of [Os3(CO)10 (CH3CN)] in THF at −78°C yields yellow crystals of [{Os3(CO)10(μ-H)}2 (O2CC6H4S)2] 1 in moderate yield. Hydrogenetaion of 1 in refluxing CHCl3 affords [Os3(CO)1(μ-H)(O2CC6H5)] 2 in good yield. Structures of 1 and 2 have been established by single crystal X-ray structure analysis.
Persistent Identifierhttp://hdl.handle.net/10722/70463
ISSN
2015 Impact Factor: 1.664
2015 SCImago Journal Rankings: 0.416

 

DC FieldValueLanguage
dc.contributor.authorLee, SMen_HK
dc.contributor.authorWong, WTen_HK
dc.date.accessioned2010-09-06T06:23:07Z-
dc.date.available2010-09-06T06:23:07Z-
dc.date.issued1996en_HK
dc.identifier.citationJournal of Cluster Science, 1996, v. 7, p. 37-47en_HK
dc.identifier.issn1040-7278en_HK
dc.identifier.urihttp://hdl.handle.net/10722/70463-
dc.description.abstractThe reaction of 2,2'-dithiosalicylic acid with two equivalents of [Os3(CO)10 (CH3CN)] in THF at −78°C yields yellow crystals of [{Os3(CO)10(μ-H)}2 (O2CC6H4S)2] 1 in moderate yield. Hydrogenetaion of 1 in refluxing CHCl3 affords [Os3(CO)1(μ-H)(O2CC6H5)] 2 in good yield. Structures of 1 and 2 have been established by single crystal X-ray structure analysis.-
dc.languageengen_HK
dc.publisherSpringer New York LLC. The Journal's web site is located at http://springerlink.metapress.com/openurl.asp?genre=journal&issn=1040-7278en_HK
dc.relation.ispartofJournal of Cluster Scienceen_HK
dc.titleOxidative addition of 2,2-dithiosalicylic acid to the cluster [Os3(CO)10(CH3CN)2]en_HK
dc.typeArticleen_HK
dc.identifier.openurlhttp://library.hku.hk:4550/resserv?sid=HKU:IR&issn=1040-7278&volume=7&spage=37&epage=47&date=1996&atitle=Oxidative+addition+of+2,2-dithiosalicylic+acid+to+the+cluster+[Os3(CO)10(CH3CN)2]en_HK
dc.identifier.emailWong, WT: wtwong@hku.hken_HK
dc.identifier.authorityWong, WT=rp00811en_HK
dc.identifier.doi10.1007/BF01166175-
dc.identifier.scopuseid_2-s2.0-21344463952-
dc.identifier.hkuros14639en_HK
dc.identifier.volume7-
dc.identifier.spage37-
dc.identifier.epage47-

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