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Article: Synthesis and X-ray crystal structures of [Ph2PMe2][(η5-C5H4But)2Li] and [(η5-C5H4But)2Yb(Cl)CH2P(Me)Ph2]

TitleSynthesis and X-ray crystal structures of [Ph2PMe2][(η5-C5H4But)2Li] and [(η5-C5H4But)2Yb(Cl)CH2P(Me)Ph2]
Authors
Issue Date1996
PublisherElsevier BV. The Journal's web site is located at http://www.elsevier.com/locate/poly
Citation
Polyhedron, 1996, v. 15 n. 24, p. 4593-4597 How to Cite?
AbstractThe interaction of [(η5-C5H4But)2YbCl · LiCl] with one equivalent of Li[(CH2) (CH2)PPh2] in tetrahydrofuran gave [Ph2PMe2][(η5-C5H4But)2Li] (1) and [(η5-C5H4But)2Yb(Cl)CH2P(Me)Ph2] (2) in 10% and 30% yields, respectively. 1 could also be prepared in 70% yield from the reaction of [Ph2PMe2][CF3SO3] with two equivalents of (C5H4But)Li. Both compounds have been fully characterized by analytical, spectroscopic and X-ray diffraction methods. The solid state structure of 1 reveals a sandwich structure for the [(η5-C5H4But)2Li]− anion.
Persistent Identifierhttp://hdl.handle.net/10722/69535
ISSN
2015 Impact Factor: 2.108
2015 SCImago Journal Rankings: 0.592
ISI Accession Number ID

 

DC FieldValueLanguage
dc.contributor.authorWong, WKen_HK
dc.contributor.authorZhang, Len_HK
dc.contributor.authorWong, WTen_HK
dc.contributor.authorXue, Fen_HK
dc.contributor.authorMak, TCWen_HK
dc.date.accessioned2010-09-06T06:14:34Z-
dc.date.available2010-09-06T06:14:34Z-
dc.date.issued1996en_HK
dc.identifier.citationPolyhedron, 1996, v. 15 n. 24, p. 4593-4597en_HK
dc.identifier.issn0277-5387en_HK
dc.identifier.urihttp://hdl.handle.net/10722/69535-
dc.description.abstractThe interaction of [(η5-C5H4But)2YbCl · LiCl] with one equivalent of Li[(CH2) (CH2)PPh2] in tetrahydrofuran gave [Ph2PMe2][(η5-C5H4But)2Li] (1) and [(η5-C5H4But)2Yb(Cl)CH2P(Me)Ph2] (2) in 10% and 30% yields, respectively. 1 could also be prepared in 70% yield from the reaction of [Ph2PMe2][CF3SO3] with two equivalents of (C5H4But)Li. Both compounds have been fully characterized by analytical, spectroscopic and X-ray diffraction methods. The solid state structure of 1 reveals a sandwich structure for the [(η5-C5H4But)2Li]− anion.-
dc.languageengen_HK
dc.publisherElsevier BV. The Journal's web site is located at http://www.elsevier.com/locate/polyen_HK
dc.relation.ispartofPolyhedronen_HK
dc.titleSynthesis and X-ray crystal structures of [Ph2PMe2][(η5-C5H4But)2Li] and [(η5-C5H4But)2Yb(Cl)CH2P(Me)Ph2]en_HK
dc.typeArticleen_HK
dc.identifier.openurlhttp://library.hku.hk:4550/resserv?sid=HKU:IR&issn=0277-5387&volume=15&issue=24&spage=4593&epage=4597&date=1996&atitle=Synthesis+and+x-ray+crystal+structures+of+[Ph2PMe2][h5=V5H4But)2Li]+and+[(h5-C5H4But)2Yb(Cl)CH2P(Me)Ph2]en_HK
dc.identifier.emailWong, WT: wtwong@hku.hken_HK
dc.identifier.authorityWong, WT=rp00811en_HK
dc.identifier.doi10.1016/0277-5387(96)00231-8-
dc.identifier.scopuseid_2-s2.0-0001321637-
dc.identifier.hkuros21852en_HK
dc.identifier.volume15-
dc.identifier.issue24-
dc.identifier.spage4593-
dc.identifier.epage4597-
dc.identifier.isiWOS:A1996VM01700035-
dc.publisher.placeNetherlands-

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