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Article: Determination of squalene using high-performance liquid chromatography with diode array detection

TitleDetermination of squalene using high-performance liquid chromatography with diode array detection
Authors
Lu, HTJiang, YChen, F
KeywordsColumn liquid chromatography
Extraction and fractional crystallization
Squalene from natural and pharmaceutical sources
Issue Date2004
PublisherFriedr Vieweg und Sohn Verlagsgesellschaft mbH. The Journal's web site is located at http://www.elsevier.com/locate/chromatographia
Citation
Chromatographia, 2004, v. 59 n. 5-6, p. 367-371 How to Cite?
AbstractA high-performance liquid chromotographic method with photodiode array detection has been developed for the determination of squalene. After treated by extraction and fractional crystallization, squalene was analyzed on a C 18 column (150 x 3.9 mm, 5 μm) with acetonitrile as mobile phase. Excellent linearity of the calibration curve was observed in the range of 100-40000 μgL-1 and the detection limit was 40 μgL -1. The recoveries were from 89.6% to 100.5% and the relative standard deviations were from 0.5% to 1.4%. The method was successfully applied to the determination of squalene in squalene capsules, olive oil, algal lipids and algal cells.
Persistent Identifierhttp://hdl.handle.net/10722/68383
ISSN
0009-5893
2021 Impact Factor: 2.213
2020 SCImago Journal Rankings: 0.427
References
References in Scopus

 

DC FieldValueLanguage
dc.contributor.authorLu, HTen_HK
dc.contributor.authorJiang, Yen_HK
dc.contributor.authorChen, Fen_HK
dc.date.accessioned2010-09-06T06:04:08Z-
dc.date.available2010-09-06T06:04:08Z-
dc.date.issued2004en_HK
dc.identifier.citationChromatographia, 2004, v. 59 n. 5-6, p. 367-371en_HK
dc.identifier.issn0009-5893en_HK
dc.identifier.urihttp://hdl.handle.net/10722/68383-
dc.description.abstractA high-performance liquid chromotographic method with photodiode array detection has been developed for the determination of squalene. After treated by extraction and fractional crystallization, squalene was analyzed on a C 18 column (150 x 3.9 mm, 5 μm) with acetonitrile as mobile phase. Excellent linearity of the calibration curve was observed in the range of 100-40000 μgL-1 and the detection limit was 40 μgL -1. The recoveries were from 89.6% to 100.5% and the relative standard deviations were from 0.5% to 1.4%. The method was successfully applied to the determination of squalene in squalene capsules, olive oil, algal lipids and algal cells.en_HK
dc.languageengen_HK
dc.publisherFriedr Vieweg und Sohn Verlagsgesellschaft mbH. The Journal's web site is located at http://www.elsevier.com/locate/chromatographiaen_HK
dc.relation.ispartofChromatographiaen_HK
dc.subjectColumn liquid chromatographyen_HK
dc.subjectExtraction and fractional crystallizationen_HK
dc.subjectSqualene from natural and pharmaceutical sourcesen_HK
dc.titleDetermination of squalene using high-performance liquid chromatography with diode array detectionen_HK
dc.typeArticleen_HK
dc.identifier.openurlhttp://library.hku.hk:4550/resserv?sid=HKU:IR&issn=0009-5893&volume=59&spage=367&epage=371&date=2004&atitle=Determination+of+squalene+using+high-performance+liquid+chromatography+with+diode+array+detectionen_HK
dc.identifier.emailChen, F: sfchen@hku.hken_HK
dc.identifier.authorityChen, F=rp00672en_HK
dc.description.naturelink_to_subscribed_fulltext-
dc.identifier.scopuseid_2-s2.0-1642443922en_HK
dc.identifier.hkuros90886en_HK
dc.relation.referenceshttp://www.scopus.com/mlt/select.url?eid=2-s2.0-1642443922&selection=ref&src=s&origin=recordpageen_HK
dc.identifier.volume59en_HK
dc.identifier.issue5-6en_HK
dc.identifier.spage367en_HK
dc.identifier.epage371en_HK
dc.publisher.placeGermanyen_HK
dc.identifier.scopusauthoridLu, HT=7404843255en_HK
dc.identifier.scopusauthoridJiang, Y=24605346600en_HK
dc.identifier.scopusauthoridChen, F=7404907980en_HK
dc.identifier.issnl0009-5893-

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