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Article: Nuclear magnetic resonance spectroscopic analysis of homoallylic and bis homoallylic substituted methyl fatty ester derivatives

TitleNuclear magnetic resonance spectroscopic analysis of homoallylic and bis homoallylic substituted methyl fatty ester derivatives
Authors
Issue Date1995
PublisherAOCS Press. The Journal's web site is located at http://www.aocs.org/press/lipids.htm
Citation
Lipids, 1995, v. 30 n. 2, p. 115-120 How to Cite?
AbstractUsing a combination of selective irradiation 1H nuclear magnetic resonance experiments and two-dimensional 1H-13C correlation spectroscopy spectral analysis of homoallylic and bis homoallylic substituted (azido, acetoxy, chloro and oxo) fatty ester derivatives, the carbon shifts of the ethylenic carbon atoms were determined. In the case of methyl 12-azido-9Z-octadecenoate (homoallylic), the carbon chemical shifts of the ethylenic C-9 and C-10 carbon nuclei are 133.092 and 124.596 ppm, respectively. In methyl 9-azido-12Z-octadecenoate (bis homoallylic), the carbon chemical shift of the ethylenic C-12 and C-13 carbon nuclei are 128.118 and 131.243 ppm, respectively.
Persistent Identifierhttp://hdl.handle.net/10722/209288
ISSN
2015 Impact Factor: 1.892
2015 SCImago Journal Rankings: 0.795

 

DC FieldValueLanguage
dc.contributor.authorJie, MSen_US
dc.contributor.authorCheng, KLen_US
dc.date.accessioned2015-04-17T05:04:10Z-
dc.date.available2015-04-17T05:04:10Z-
dc.date.issued1995en_US
dc.identifier.citationLipids, 1995, v. 30 n. 2, p. 115-120en_US
dc.identifier.issn0024-4201en_US
dc.identifier.urihttp://hdl.handle.net/10722/209288-
dc.description.abstractUsing a combination of selective irradiation 1H nuclear magnetic resonance experiments and two-dimensional 1H-13C correlation spectroscopy spectral analysis of homoallylic and bis homoallylic substituted (azido, acetoxy, chloro and oxo) fatty ester derivatives, the carbon shifts of the ethylenic carbon atoms were determined. In the case of methyl 12-azido-9Z-octadecenoate (homoallylic), the carbon chemical shifts of the ethylenic C-9 and C-10 carbon nuclei are 133.092 and 124.596 ppm, respectively. In methyl 9-azido-12Z-octadecenoate (bis homoallylic), the carbon chemical shift of the ethylenic C-12 and C-13 carbon nuclei are 128.118 and 131.243 ppm, respectively.en_US
dc.languageengen_US
dc.publisherAOCS Press. The Journal's web site is located at http://www.aocs.org/press/lipids.htmen_US
dc.relation.ispartofLipidsen_US
dc.titleNuclear magnetic resonance spectroscopic analysis of homoallylic and bis homoallylic substituted methyl fatty ester derivativesen_US
dc.typeArticleen_US
dc.identifier.emailJie, MS: hrsclkj@hku.hken_US
dc.description.naturelink_to_subscribed_fulltext-
dc.identifier.doi10.1007/BF02538263en_US
dc.identifier.pmid7769966en_US
dc.identifier.hkuros511en_US
dc.identifier.volume30en_US
dc.identifier.issue2en_US
dc.identifier.spage115en_US
dc.identifier.epage120en_US
dc.publisher.placeUnited Statesen_US

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