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Article: Determination of triphenyltin and its metabolite diphenyltin in culture medium by high-performance liquid chromatography with UV detection

TitleDetermination of triphenyltin and its metabolite diphenyltin in culture medium by high-performance liquid chromatography with UV detection
Authors
KeywordsColumn Liquid Chromatography
Culture Medium
Diphenyltin
Triphenyltin
Issue Date2004
PublisherFriedr Vieweg und Sohn Verlagsgesellschaft mbH. The Journal's web site is located at http://www.elsevier.com/locate/chromatographia
Citation
Chromatographia, 2004, v. 60 n. 1-2, p. 113-116 How to Cite?
AbstractA method for the determination of triphenyltin and diphenyltin was developed by reversed-phase high-performance liquid chromatography with UV detection. Triphenyltin and diphenyltin were separated using a reversed-phase Symmetry C18 column (150 x 3.9 mm, 5 μm) with tetrahydrofuran- water-acetonitrile-glacial acetic acid (13:25:5:7, v/v) containing 0.05% triethylamine and 1.0% sodium acetate as mobile phase at 0.50 mL min -1 and detection at 257 nm. The calibration curves were linear from 0.26 μmol L-1 to 1100 μmol L-1 for triphenyltin with a correlation coefficient of 0.9999 (n = 12) and from 0.60 μmol L -1 to 1200 μmol L-1 for diphenyltin with a correlation coefficient of 0.9991 (n = 12), respectively. The detection limits of triphenyltin and diphenyltin were 0.2 μmol L-1, respectively. The method was successfully applied to the determination of triphenyltin and its metabolite diphenyltin in culture medium. The recoveries of triphenyltin and diphenyltin were in the ranges of 97.7% to 103.3% and 85.5% to 91.6%, respectively.
Persistent Identifierhttp://hdl.handle.net/10722/179041
ISSN
2015 Impact Factor: 1.332
2015 SCImago Journal Rankings: 0.480
ISI Accession Number ID
References

 

DC FieldValueLanguage
dc.contributor.authorLu, HTen_US
dc.contributor.authorLi, HBen_US
dc.contributor.authorChen, Fen_US
dc.contributor.authorWong, MHen_US
dc.contributor.authorJiang, Yen_US
dc.date.accessioned2012-12-19T09:51:36Z-
dc.date.available2012-12-19T09:51:36Z-
dc.date.issued2004en_US
dc.identifier.citationChromatographia, 2004, v. 60 n. 1-2, p. 113-116en_US
dc.identifier.issn0009-5893en_US
dc.identifier.urihttp://hdl.handle.net/10722/179041-
dc.description.abstractA method for the determination of triphenyltin and diphenyltin was developed by reversed-phase high-performance liquid chromatography with UV detection. Triphenyltin and diphenyltin were separated using a reversed-phase Symmetry C18 column (150 x 3.9 mm, 5 μm) with tetrahydrofuran- water-acetonitrile-glacial acetic acid (13:25:5:7, v/v) containing 0.05% triethylamine and 1.0% sodium acetate as mobile phase at 0.50 mL min -1 and detection at 257 nm. The calibration curves were linear from 0.26 μmol L-1 to 1100 μmol L-1 for triphenyltin with a correlation coefficient of 0.9999 (n = 12) and from 0.60 μmol L -1 to 1200 μmol L-1 for diphenyltin with a correlation coefficient of 0.9991 (n = 12), respectively. The detection limits of triphenyltin and diphenyltin were 0.2 μmol L-1, respectively. The method was successfully applied to the determination of triphenyltin and its metabolite diphenyltin in culture medium. The recoveries of triphenyltin and diphenyltin were in the ranges of 97.7% to 103.3% and 85.5% to 91.6%, respectively.en_US
dc.languageengen_US
dc.publisherFriedr Vieweg und Sohn Verlagsgesellschaft mbH. The Journal's web site is located at http://www.elsevier.com/locate/chromatographiaen_US
dc.relation.ispartofChromatographiaen_US
dc.subjectColumn Liquid Chromatographyen_US
dc.subjectCulture Mediumen_US
dc.subjectDiphenyltinen_US
dc.subjectTriphenyltinen_US
dc.titleDetermination of triphenyltin and its metabolite diphenyltin in culture medium by high-performance liquid chromatography with UV detectionen_US
dc.typeArticleen_US
dc.identifier.emailChen, F: sfchen@hku.hken_US
dc.identifier.authorityChen, F=rp00672en_US
dc.description.naturelink_to_subscribed_fulltexten_US
dc.identifier.doi10.1365/s10337-004-0328-3-
dc.identifier.scopuseid_2-s2.0-3943060823en_US
dc.identifier.hkuros105988-
dc.relation.referenceshttp://www.scopus.com/mlt/select.url?eid=2-s2.0-3943060823&selection=ref&src=s&origin=recordpageen_US
dc.identifier.volume60en_US
dc.identifier.issue1-2en_US
dc.identifier.spage113en_US
dc.identifier.epage116en_US
dc.identifier.isiWOS:000224100500020-
dc.publisher.placeGermanyen_US
dc.identifier.scopusauthoridLu, HT=7404843255en_US
dc.identifier.scopusauthoridLi, HB=25649944400en_US
dc.identifier.scopusauthoridChen, F=7404907980en_US
dc.identifier.scopusauthoridWong, MH=7403908633en_US
dc.identifier.scopusauthoridJiang, Y=24605346600en_US

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