File Download
There are no files associated with this item.
Links for fulltext
(May Require Subscription)
- Publisher Website: 10.1365/s10337-004-0328-3
- Scopus: eid_2-s2.0-3943060823
- WOS: WOS:000224100500020
- Find via
Supplementary
- Citations:
- Appears in Collections:
Article: Determination of triphenyltin and its metabolite diphenyltin in culture medium by high-performance liquid chromatography with UV detection
Title | Determination of triphenyltin and its metabolite diphenyltin in culture medium by high-performance liquid chromatography with UV detection |
---|---|
Authors | |
Keywords | Column Liquid Chromatography Culture Medium Diphenyltin Triphenyltin |
Issue Date | 2004 |
Publisher | Friedr Vieweg und Sohn Verlagsgesellschaft mbH. The Journal's web site is located at http://www.elsevier.com/locate/chromatographia |
Citation | Chromatographia, 2004, v. 60 n. 1-2, p. 113-116 How to Cite? |
Abstract | A method for the determination of triphenyltin and diphenyltin was developed by reversed-phase high-performance liquid chromatography with UV detection. Triphenyltin and diphenyltin were separated using a reversed-phase Symmetry C18 column (150 x 3.9 mm, 5 μm) with tetrahydrofuran- water-acetonitrile-glacial acetic acid (13:25:5:7, v/v) containing 0.05% triethylamine and 1.0% sodium acetate as mobile phase at 0.50 mL min -1 and detection at 257 nm. The calibration curves were linear from 0.26 μmol L-1 to 1100 μmol L-1 for triphenyltin with a correlation coefficient of 0.9999 (n = 12) and from 0.60 μmol L -1 to 1200 μmol L-1 for diphenyltin with a correlation coefficient of 0.9991 (n = 12), respectively. The detection limits of triphenyltin and diphenyltin were 0.2 μmol L-1, respectively. The method was successfully applied to the determination of triphenyltin and its metabolite diphenyltin in culture medium. The recoveries of triphenyltin and diphenyltin were in the ranges of 97.7% to 103.3% and 85.5% to 91.6%, respectively. |
Persistent Identifier | http://hdl.handle.net/10722/179041 |
ISSN | 2023 Impact Factor: 1.2 2023 SCImago Journal Rankings: 0.301 |
ISI Accession Number ID | |
References |
DC Field | Value | Language |
---|---|---|
dc.contributor.author | Lu, HT | en_US |
dc.contributor.author | Li, HB | en_US |
dc.contributor.author | Chen, F | en_US |
dc.contributor.author | Wong, MH | en_US |
dc.contributor.author | Jiang, Y | en_US |
dc.date.accessioned | 2012-12-19T09:51:36Z | - |
dc.date.available | 2012-12-19T09:51:36Z | - |
dc.date.issued | 2004 | en_US |
dc.identifier.citation | Chromatographia, 2004, v. 60 n. 1-2, p. 113-116 | en_US |
dc.identifier.issn | 0009-5893 | en_US |
dc.identifier.uri | http://hdl.handle.net/10722/179041 | - |
dc.description.abstract | A method for the determination of triphenyltin and diphenyltin was developed by reversed-phase high-performance liquid chromatography with UV detection. Triphenyltin and diphenyltin were separated using a reversed-phase Symmetry C18 column (150 x 3.9 mm, 5 μm) with tetrahydrofuran- water-acetonitrile-glacial acetic acid (13:25:5:7, v/v) containing 0.05% triethylamine and 1.0% sodium acetate as mobile phase at 0.50 mL min -1 and detection at 257 nm. The calibration curves were linear from 0.26 μmol L-1 to 1100 μmol L-1 for triphenyltin with a correlation coefficient of 0.9999 (n = 12) and from 0.60 μmol L -1 to 1200 μmol L-1 for diphenyltin with a correlation coefficient of 0.9991 (n = 12), respectively. The detection limits of triphenyltin and diphenyltin were 0.2 μmol L-1, respectively. The method was successfully applied to the determination of triphenyltin and its metabolite diphenyltin in culture medium. The recoveries of triphenyltin and diphenyltin were in the ranges of 97.7% to 103.3% and 85.5% to 91.6%, respectively. | en_US |
dc.language | eng | en_US |
dc.publisher | Friedr Vieweg und Sohn Verlagsgesellschaft mbH. The Journal's web site is located at http://www.elsevier.com/locate/chromatographia | en_US |
dc.relation.ispartof | Chromatographia | en_US |
dc.subject | Column Liquid Chromatography | en_US |
dc.subject | Culture Medium | en_US |
dc.subject | Diphenyltin | en_US |
dc.subject | Triphenyltin | en_US |
dc.title | Determination of triphenyltin and its metabolite diphenyltin in culture medium by high-performance liquid chromatography with UV detection | en_US |
dc.type | Article | en_US |
dc.identifier.email | Chen, F: sfchen@hku.hk | en_US |
dc.identifier.authority | Chen, F=rp00672 | en_US |
dc.description.nature | link_to_subscribed_fulltext | en_US |
dc.identifier.doi | 10.1365/s10337-004-0328-3 | - |
dc.identifier.scopus | eid_2-s2.0-3943060823 | en_US |
dc.identifier.hkuros | 105988 | - |
dc.relation.references | http://www.scopus.com/mlt/select.url?eid=2-s2.0-3943060823&selection=ref&src=s&origin=recordpage | en_US |
dc.identifier.volume | 60 | en_US |
dc.identifier.issue | 1-2 | en_US |
dc.identifier.spage | 113 | en_US |
dc.identifier.epage | 116 | en_US |
dc.identifier.isi | WOS:000224100500020 | - |
dc.publisher.place | Germany | en_US |
dc.identifier.scopusauthorid | Lu, HT=7404843255 | en_US |
dc.identifier.scopusauthorid | Li, HB=25649944400 | en_US |
dc.identifier.scopusauthorid | Chen, F=7404907980 | en_US |
dc.identifier.scopusauthorid | Wong, MH=7403908633 | en_US |
dc.identifier.scopusauthorid | Jiang, Y=24605346600 | en_US |
dc.identifier.issnl | 0009-5893 | - |