Enamel microhardness and bond strengths of self-etching primer adhesives

Abstract

The aim of this study was to determine the relationship between enamel surface microhardness and microshear bond strength (μSBS). Buccal and lingual mid-coronal enamel sections were prepared from 22 permanent human molars and divided into two groups, each comprising the buccal and lingual enamel from 11 teeth, to analyze two self-etching primer adhesives (Clearfil SE Bond and Tokuyama Bond Force). One-half of each enamel surface was tested using the Vickers hardness test with 10 indentations at 1 N and a 15-s dwell time. A hybrid resin composite was bonded to the other half of the enamel surface with the adhesive system assigned to the group. After 24 h of water storage of specimens at 37o°C, the μSBS test was carried out on a universal testing machine at a crosshead speed of 1 mm min-1 until bond failure occurred. The mean μSBS was regressed on the mean Vickers hardness number (VHN) using a weighted regression analysis in order to explore the relationship between enamel hardness and μSBS. The weights used were the inverse of the variance of the μSBS means. Neither separate correlation analyses for each adhesive nor combined regression analyses showed a significant correlation between the VHN and the μSBS. These results suggest that the μSBS of the self-etch adhesive systems are not influenced by enamel surface microhardness. © 2010 The Authors. Journal compilation © 2010 Eur J Oral Sci.