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Article: Tetrahedral mixed-metal clusters containing bridging sulfido ligands. Synthesis and crystal and molecular structures of PtOs3(CO)8(PMe2Ph)3(μ 3-S) and Os3W(CO)11(PMe2Ph)2(μ 3-S)

TitleTetrahedral mixed-metal clusters containing bridging sulfido ligands. Synthesis and crystal and molecular structures of PtOs3(CO)8(PMe2Ph)3(μ 3-S) and Os3W(CO)11(PMe2Ph)2(μ 3-S)
Authors
Issue Date1984
Citation
Organometallics, 1984, v. 3, n. 4, p. 634-636 How to Cite?
AbstractThe new tetrahedral mixed-metal cluster compounds PtOs3(CO)8(PMe2Ph)3(μ 3-S) (2) and Os3W-(CO)11(PMe2Ph)2(μ 3-S) (4) have been prepared by the reaction of Os3(CO)10(μ3-S) (1) with Pt(PMe2Ph)4 upon mixing at room temperature and with W(CO)5(PMe2Ph) in the presence of UV irradiation in yields of 26% and 27%, respectively, and have been characterized by single-crystal X-ray diffraction methods. © 1984 American Chemical Society.
Persistent Identifierhttp://hdl.handle.net/10722/219524
ISSN
2015 Impact Factor: 4.186
2015 SCImago Journal Rankings: 2.043

 

DC FieldValueLanguage
dc.contributor.authorAdams, Richard D.-
dc.contributor.authorHor, T. S Andy-
dc.contributor.authorMathur, Pradeep-
dc.date.accessioned2015-09-23T02:57:18Z-
dc.date.available2015-09-23T02:57:18Z-
dc.date.issued1984-
dc.identifier.citationOrganometallics, 1984, v. 3, n. 4, p. 634-636-
dc.identifier.issn0276-7333-
dc.identifier.urihttp://hdl.handle.net/10722/219524-
dc.description.abstractThe new tetrahedral mixed-metal cluster compounds PtOs3(CO)8(PMe2Ph)3(μ 3-S) (2) and Os3W-(CO)11(PMe2Ph)2(μ 3-S) (4) have been prepared by the reaction of Os3(CO)10(μ3-S) (1) with Pt(PMe2Ph)4 upon mixing at room temperature and with W(CO)5(PMe2Ph) in the presence of UV irradiation in yields of 26% and 27%, respectively, and have been characterized by single-crystal X-ray diffraction methods. © 1984 American Chemical Society.-
dc.languageeng-
dc.relation.ispartofOrganometallics-
dc.titleTetrahedral mixed-metal clusters containing bridging sulfido ligands. Synthesis and crystal and molecular structures of PtOs3(CO)8(PMe2Ph)3(μ 3-S) and Os3W(CO)11(PMe2Ph)2(μ 3-S)-
dc.typeArticle-
dc.description.natureLink_to_subscribed_fulltext-
dc.identifier.scopuseid_2-s2.0-33750254416-
dc.identifier.volume3-
dc.identifier.issue4-
dc.identifier.spage634-
dc.identifier.epage636-

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